Fundamental Experiments in Materials Chemistry 2

Course Information

College Anan College Year 2024
Course Title Fundamental Experiments in Materials Chemistry 2
Course Code 1412T21 Course Category Specialized / Compulsory
Class Format Experiment / Practical training Credits School Credit: 2
Department Course of Chemical Engineering Student Grade 2nd
Term Second Semester Classes per Week 後期:4
Textbook and/or Teaching Materials Handout (Fundamental Experiments in Materials Chemistry 1), Fundamentals of Chemistry (Daiichi Gakushu-sha), Chemistry (Daiichi Gakushu-sha)
Instructor Sugiyama Yuuki,Otani Takashi

Course Objectives

1. The students will learn how to prepare reports using experimental data.
2. The students will use experimental methods to synthesize organic compounds (assembly of experimental apparatus, weighing and mixing of reagents, adjustment of reaction conditions, post-reaction treatment, isolation and purification of products).
3. The students will use methods to confirm (identify) products of organic compounds.

Rubric

Ideal LevelStandard LevelMinimum Level
Objective 1The student will prepare a logical and appropriate report using the experimental data.The student will prepare a logical report using the experimental data.The student will prepare a report using the experimental data.
Objective 2The student will properly perform synthetic experiments on organic compounds.The student will perform synthetic experiments on organic compounds.The student will conduct synthetic experiments of organic compounds with instructions.
Objective 3The students will adequately identify the products of organic compounds.The students will identify the products of organic compounds.The students identify the products of organic compounds with instructions.

Assigned Department Objectives

学習・教育到達度目標 D-2 See Hide
学習・教育到達度目標 D-4 See Hide

Teaching Method

Outline:
To understand and master chemistry as an academic discipline, it is essential to take classes in each specialized subject and conduct experiments in chemistry. This course is the first experimental course for students after they are assigned to the Chemistry Course. It aims to provide basic knowledge of chemistry experiments (experimental techniques, rules of chemistry laboratories, how to prepare laboratory notebooks, how to discuss experimental results, etc.).
To learn basic organic chemistry experimental operations (assembly of experimental apparatus, weighing and mixing of reagents, adjustment of reaction conditions, post-treatment of reactions, isolation, and purification of products) and methods to check products by performing typical organic chemistry reactions. Understand the meaning of experimental manipulations and reaction mechanisms, and be able to prepare logical reports of experimental results.
Style:
Experiments are the foundation of chemistry, and mastery of basic techniques is essential. Students will first consider the purpose of the experiment, learn experimental methods and concepts in the preliminary study, and then confirm them in the experiment to experience and deepen their understanding of the laws of chemistry. After the experiments, students analyze the experimental data obtained through accurate measurements and compile them into a report. If this report writing phase is considered a review, the students will learn the experiment in depth by repeating the chemistry experiment's preparation, experiment, and review phases. Students must complete the experimental plan in the experimental notebook before the experiment begins. At the end of the experiment, students must submit the notebook and report the results and experimental data to the instructor in charge to complete this experiment.
Notice:
The following precautions must be taken to ensure the experiment is carried out safely.

1. Eating and drinking are strictly prohibited in the laboratory.
2. Students must wear the prescribed white lab coat and jacket when entering the laboratory. Students with long hair must tie it back.
3. Before starting experiments, students must wear safety glasses and gloves.
4. Students must promptly follow any instructions given by the teacher.
5. Reports must be submitted by the due date.
6. In case of absence, notify the teacher immediately. No credit will be given for any unexperienced work or reports that have yet to be submitted.
7. Grades will be based on reports, notes, examinations, and attitude.

Characteristics of Class / Division in Learning

Active Learning
Aided by ICT
Applicable to Remote Class
Instructor Professionally Experienced

Course Plan

Theme Goals
2nd Semester
3rd Quarter
1st Guidance
2nd Separation and purification of organic compounds (1) Purify by recrystallization
3rd Synthesis of superabsorbent polymer (1) Synthesize cross-linkable polymer.
4th Synthesis of superabsorbent polymer (2) Evaluate the water absorption of synthesized polymers.
5th Synthesis of ethyl acetate (1) Synthesize ester.
6th Synthesis of ethyl acetate (2) Perform fractional distillation, GC, and NMR measurements to identify ethyl acetate.
7th IR, NMR analysis method Explain and analyze the principles of IR and NMR.
8th Separation and purification of organic compounds (2) Extraction is performed using a separatory funnel.
4th Quarter
9th Synthesis of acetanilide (1) Synthesize amide.
10th Synthesis of acetanilide (2) IR, NMR, and melting point measurements are performed to identify acetanilide.
11th Report coaching and lectures
12th Interfacial polycondensation reaction Synthesize 66 nylon.
13th Synthesis of azo dyes (1) Synthesize azo compound by azo coupling.
14th Synthesis of azo dyes (2) Identify compounds by TLC.
15th Instrument Check, examination, submission of notes, and summary of experiments
16th Preliminary Experiment Day/Instrument Check

Evaluation Method and Weight (%)

ExaminationQuizPortfolioPresentation and AttitudeOtherTotal
Subtotal0000100100
Basic Proficiency00006060
Specialized Proficiency00004040
Cross Area Proficiency000000